Design and characterization of a rapid response system based on piezoelectric detection
DOI:
https://doi.org/10.54139/revinguc.v28i3.43Keywords:
piezoelectricity, Quartz Crystal Microbalance (QCM), rapid response systemsAbstract
Analytical arrangements based on quartz crystal microbalances are currently of great importance as they are techniques for the rapid qualitative or quantitative determination of chemical species, as well as allowing monitoring of the analysis in situ in real time. The present study presents the design and characterization of a rapid response measurement system based on piezoelectric detection. For its elaboration, an oscillatory circuit was built, a home-made type using a piezoelectric crystal with a cut-off frequency of 10 MHz as a means of detection.Measurements were made in the equipment without solvent and without analyte in order to verify the manufacturing cutoff resonance frequency and later using volumes of 10 and 20 µL for the solvent and saline solutions in order to verify their analytical response.The calibration curve obtained showed a linear behavior comprised in the range of (0.005 - 0.050) % w/v of NaCl with a correlation coefficient of 0.9219 and a precision expressed by the relative standard deviation (RSD) of 0.8124. The results allow to establish that the proposed instrumental development can be used satisfactorily in methodologies that require immediate response, high sensitivity and low sample volume.
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